[1]张翔,魏浩栋,姚纪蕾,等.单分散尺寸可控的聚苯乙烯微球的制备[J].郑州大学学报(工学版),2014,35(05):105-108.[doi:10.3969/j.issn.1671 -6833.2014.05.024]
ZHANG Xiang,WEI Haodong,YA0 Jilei.Preparation of Monodisperse Size-controlled Polystyrene Microspheres by Dispersion Polymerization[J].Journal of Zhengzhou University (Engineering Science),2014,35(05):105-108.[doi:10.3969/j.issn.1671 -6833.2014.05.024]
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单分散尺寸可控的聚苯乙烯微球的制备()
《郑州大学学报(工学版)》[ISSN:1671-6833/CN:41-1339/T]
- 卷:
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35
- 期数:
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2014年05期
- 页码:
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105-108
- 栏目:
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- 出版日期:
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2014-09-30
文章信息/Info
- Title:
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Preparation of Monodisperse Size-controlled Polystyrene Microspheres by Dispersion Polymerization
- 作者:
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张翔; 魏浩栋; 姚纪蕾; 张冰
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- Author(s):
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ZHANG Xiang; WEI Haodong; YA0 Jilei
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School of Chemical Engineering and Energy, Zhengzhou University, Zhengzhou 450001 ,China
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- Keywords:
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polyslyrene mierosphere ; dispersion polymerization; monodisperse; size distribution
- 分类号:
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TQ317
- DOI:
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10.3969/j.issn.1671 -6833.2014.05.024
- 文献标志码:
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A
- Abstract:
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Monodisperse size-controlled polystyrene mierospheres were prepared by dispersion polymerizationof styrene in ethanol dispersion medium, using PVP as a stabilizer and AlBN as the initiator. The inlueneefaclors, such as monomer coneentration , stabilizer coneeniralion , iniliator eoneentration and reaction temperature on the size and size distribution were invesligated. The morphology and size of PSt mierospheres was charaeterized by SEM , partiele size analyzer and oplieal mieroseope. And the Fourier transorm infrared ( FTlR )spectra of PSt mierospheres were also reeorded by a FTlR speelrometer. The results showed that monodispersePSt mierospheres in the size of 3.55 pm with smooth surlaee were prepared when the monomer coneentration is22%, slabilizer PVP is 0.65% , iniliator AlBN is 0.32% and reaelion temperalure is 70 ℃.
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