[1]刘新红,刘志芳,黄亚磊,等.同轴静电纺丝制备聚乳酸-聚己内酯核-壳结构复合纤维[J].郑州大学学报(工学版),2015,36(05):20.[doi:10.3969/ j.issn.1671 -6833.2015.05.005]
SI Jun-hui,CUI Zhi-xiang,LIU Qiong,et al.Fabrication of PLA-PCL Composite Nanofiber withCore-shell Structure Through Electrospinning[J].Journal of Zhengzhou University (Engineering Science),2015,36(05):20.[doi:10.3969/ j.issn.1671 -6833.2015.05.005]
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同轴静电纺丝制备聚乳酸-聚己内酯核-壳结构复合纤维()
《郑州大学学报(工学版)》[ISSN:1671-6833/CN:41-1339/T]
- 卷:
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36
- 期数:
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2015年05期
- 页码:
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20
- 栏目:
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- 出版日期:
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2015-11-29
文章信息/Info
- Title:
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Fabrication of PLA-PCL Composite Nanofiber withCore-shell Structure Through Electrospinning
- 作者:
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刘新红; 刘志芳; 黄亚磊; 马腾司军辉; 崔志香
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1.郑州大学材料科学与工程学院,河南郑州450001;2.福建工程学院材料科学与工程学院,福建福州350118
- Author(s):
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SI Jun-hui1; 2; CUI Zhi-xiang2; LIU Qiong3; WANG Qian-ting1
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1.School of Materials Science and Engineering, Zhengzhou University ,Zhengzhou 450001 , China; 2. School of Materials Seci-ence and Engineering .Fujian University of Technology.Fuzhou 350118 ,China
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- 关键词:
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同轴静电纺丝; 核–壳结构; 聚乳酸(PLA); 聚己内酯(PCL); 复合纤维
- Keywords:
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co-axial electrospinning; core-shell structure; polylactic acid ( PLA ) ; polycaprolactone ( PCL); composite fiber
- 分类号:
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TQ342
- DOI:
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10.3969/ j.issn.1671 -6833.2015.05.005
- 文献标志码:
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A
- 摘要:
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采用同轴静电纺丝技术制备聚乳酸(PLA)-聚己内酯(PCL)核–壳结构复合纤维.利用扫描电子显微镜(SEM)观察纺丝电压、收集距离和核层-壳层溶液推进速度对PLA-PCL核–壳结构复合纤维形貌的影响.通过透射扫描电子显微镜(TEM)分析核层–壳层溶液推进速度对PLA-PCL核–壳结构形成的影响.研究结果表明:当核–壳溶液推进速度为0.1 -0.2和0.1 -0.3 mL/h时形成了清晰的核-壳结构;随着壳层溶液推进速度加快,PLA-PCL复合纤维核层含量降低,增加纺丝电压能够有效地降低复合纤维平均直径,而增大收集距离使复合纤维平均直径先降低后增加.
- Abstract:
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In this study,polylactic acid ( PLA )-polycaprolactone ( PCL) composite fiber with core-shell struc-ture was fabricated by means of co-axial electrospinning. SEM was employed to study the impacts of electro-spinning voltage,collected distance and ratio of core-shell solution injection speed on morphology of PLA-PCI.composite fiber with core-shell structure. The influences on the formation of the core-shell structure under dif-ferent ratio of core-shell solution injection speed were observed with TEM. The results showed that the obviouscore-shell structure was fabricated when core-shell solution injection speed was 0. 1-0.2 and 0.1-0.3 mL/h.The core component in PLA-PCL composite fiber decreases with the increase of shell solution injection speed.The increasing of electrospinning voltage could efficiently reduce the average diameter of composite fiber. Theaverage diameter of composite nanofiber decreases and then increases with the increase of collection distance.
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