[1]赵建宏,李磊,武红旗,等.高效液相色谱法测定叠氮磷酸二苯酯(DPPA)的含量[J].郑州大学学报(工学版),2008,29(01):21-23.
　ZHAO Jianhong,LI Lei,Wu Hongqi,et al.Determination of diphenyl azide phosphate (DPPA) by high performance liquid chromatography[J].Journal of Zhengzhou University (Engineering Science),2008,29(01):21-23.
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高效液相色谱法测定叠氮磷酸二苯酯(DPPA)的含量()
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《郑州大学学报(工学版)》[ISSN:1671-6833/CN:41-1339/T]

卷:
29
期数:
2008年01期
页码:
21-23
栏目:
出版日期:
1900-01-01

文章信息/Info

Title:
Determination of diphenyl azide phosphate (DPPA) by high performance liquid chromatography
作者:
赵建宏; 李磊; 武红旗; 等.
郑州大学,化工学院,河南,郑州,450001, 郑州大学,化工学院,河南,郑州,450001, 郑州大学,化工学院,河南,郑州,450001, 郑州大学,化工学院,河南,郑州,450001, 郑州大学,化工学院,河南,郑州,450001
Author(s):
ZHAO Jianhong; LI Lei; Wu Hongqi; etc
关键词:
高效液相色谱;  叠氮磷酸二苯酯;  相转移催化
Keywords:
文献标志码:
A
摘要:
采用高效液相色谱法,紫外检测器(检测波长254 nm),在C18(150 mm × 4.6 mm i.d.)色谱柱上,以V(甲醇)∶ V(水)=70∶ 30为流动相,对由氯代磷酸二苯酯和叠氮钠为原料,相转移催化法合成的DPPA进行定量分析.结果表明,该方法的相对标准偏差为0.3 %,平均回收率99.60 %,线性相关系数为0.999 9.
Abstract:

Using high performance liquid chromatography, UV detector (detection wavelength 254 nm), at C18 (150 mm × 4.6 mm i.d.) On the column, the DPPA synthesized by phase transfer catalysis using V(methanol)∶V(water)=70∶ 30 as mobile phase was used as mobile phase. The results showed that the relative standard deviation of the method was 0.3%, the average recovery was 99.60%, and the linear correlation coefficient was 0.999 9.

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更新日期/Last Update: 1900-01-01